Performance Evaluation of Analytical Equipment PDF Print E-mail

This briefing note provides details of ISO 10723:1995- Natural gas – Performance evaluation for on-line analytical systems

EffecTech uses this standard to quantify the performance characteristics of your instrument in conjunction with their UKAS site accreditation according to ISO 17025.

Why do I need a quantitative performance test?

  • To improve energy efficiency costs
  • To conform with EU emissions trading legislation
  • To validate your analytical system
  • To highlight instrument limitations
  • To reduce potential financial exposure

EffecTech uses instrument performance characteristics to

  • Set analytical specifications
  • Design the most appropriate calibration gas composition
  • Determine the bias and uncertainty of the analytical system

 

What is ISO 10723?

The standard (ISO 10723:1995 - Natural gas - Performance evaluation for on-line analytical systems) was issued in December 1995 by ISO Technical Committee 193.

EffecTech personnel were responsible for writing and testing major parts of the standard. Subsequently, through practical experience, they have refined the procedures for carrying out the tests and processing the raw data produced.

Applying the standard gives you measures of performance which can be compared with a specification or benchmark which has been set previously.

It does not tell you whether the instrument is fit for purpose.

 

Objective

The objective of the performance evaluation is to give a measure of the instrument’s performance in terms of

  • Component separation
  • Repeatability of measurement
  • Maximum bias errors

 

Principle

The analytical system is set up according to the manufacturer’s / supplier’s instructions for installation and operation. The system is examined by analysing test gases, each made up of a mixture of components typically found in natural gas, with compositions covering a range wider than that for which the system has been specified.

The test gases, prepared according to an appropriate standard, are injected into the analyser to test

  • The ability of the system to measure the components specified in the analytical method (system efficiency)
  • The repeatability of the measurement of individual components over their specified range
  • The relationship between response and concentration of individual components over their specified range
  • The absence of interference between components at different concentration ratios.

Accuracy of measurement is not included in this list, as it is principally controlled by the accuracy with which the calibration gas composition is known.

 

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Summary

If the performance evaluation shows the system to be unfit for its intended purpose, then all stages of the process

  • Analytical requirement
  • Analytical procedure
  • Choice of equipment
  • Choice of calibration gas
  • The calculation procedure

must be re-examined to assess how improvements can be made.

If any modifications are made to the analytical system then the entire performance test procedure must be reapplied.

Performance evaluation of an analytical system should be performed at installation and then at regular intervals, depending on the application, and when any critical component of the analytical system is changed.

News

18 May 2012 - EffecTech will be calibrating the gas measurement system on Shell's new floating behemoth, "Prelude" the largest floating object ever created.


11 May 2012 - 120 samples for OMV Petrom in Romania completed


2 March 2012 - Qatari Lab now ISO 17025 for Calibration & Testing


18 November 2011 - Handover of new warehouse and laboratory facilities.


Our Clients

Shell BP
Tata Steel E-on
Centrica Mobil
South Hook EDF Energy


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